ICS

97.195；19.020

CCS

Y04

中華人民共和國國家標準

GB/T44202—2024

館藏絲織品老化程度測試樣品制備

Samplepreparationfortestingagingdegreeofsilktextileinmuseumcollections

2024-07-24發布2024-11-01實施

國家市場監督管理總局發布

國家標準化管理委員會

GB/T44202—2024

目次

前言

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Ⅲ

1

范圍

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1

2

規范性引用文件

······················································································

1

3

術語和定義

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1

4

取樣

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1

4.1

取樣計劃

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1

4.2

取樣過程

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1

5

樣品處理

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2

5.1

樣品清洗

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2

5.2

樣品調濕

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2

6

樣品制備

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2

7

樣品信息登記

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2

附錄A（資料性）

館藏絲織品取樣信息記錄表樣式

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3

附錄B（資料性）

館藏絲織品老化程度測試樣品信息表樣式

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4

參考文獻

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5

Ⅰ

GB/T44202—2024

前言

本文件按照GB/T1.1—2020《標準化工作導則第1部分：標準化文件的結構和起草規則》的規定

起草。

請注意本文件的某些內容可能涉及專利。本文件的發布機構不承擔識別專利的責任。

本文件由中華人民共和國國家文物局提出。

本文件由全國文物保護標準化技術委員會（SAC/TC289）歸口。

本文件起草單位：中國科學技術大學、中國國家博物館、福建理工大學、北京中科標準科技集團有

限公司。

本文件主要起草人：龔鈺軒、龔德才、鐵付德、王志民、成維智、周光昭、喬成全、胡霜晴、

鐘博超、張曉寧、王開、羅賢娟。

Ⅲ

GB/T44202—2024

館藏絲織品老化程度測試樣品制備

1范圍

本文件規定了館藏絲織品老化程度測試樣品的取樣、處理、制備、樣品信息登記等要求。

本文件適用于館藏絲織品老化程度分析中氨基酸分析、掃描電子顯微鏡、熱重分析、傅里葉變換紅

外光譜、X射線粉末衍射測試方法的樣品制備。

2規范性引用文件

下列文件中的內容通過文中的規范性引用而構成本文件必不可少的條款。其中，注日期的引用文

件，僅該日期對應的版本適用于本文件；不注日期的引用文件，其最新版本（包括所有的修改單）適用

于本文件。

GB/T6529—2008紡織品調濕和試驗用標準大氣

GB/T13464—2008物質熱穩定性的熱分析試驗方法

GB/T23863—2009博物館照明設計規范

GB/T32016—2015蠶絲氨基酸的測定

JGJ66—2015博物館建筑設計規范

3術語和定義

GB/T6529—2008界定的以及下列術語和定義適用于本文件。

3.1

絲織品老化程度agingdegreeofsilktextile

與新鮮蠶絲相比，館藏絲織品受損后所產生的微觀結構和宏觀性能變化的水平。

4取樣

4.1取樣計劃

館藏絲織品老化程度測試樣品（以下簡稱“樣品”，包括待測樣品和參比樣品1））制備應與文物的

負責單位協商后根據取樣目的制定取樣計劃，取樣計劃的相關要求如下：

a）應充分考慮歷次保護修復使用的材料和工藝對測試產生的影響；

b）根據需要和文物等級、保存狀況、病害、組織結構等特點，確定取樣位置、取樣數量、取樣量

（如樣品尺寸、樣品面積和樣品質量）、取樣方法、樣品包裝和保存方法等；

c）優先從殘件（片）或對文物價值信息（如花紋、圖案等）影響較小的地方取樣；

d）確定樣品測試后剩余樣品的處置方式（如歸還原文物負責單位、自己留存等）。

4.2取樣過程